Gazi ya Chromatografi ya Mass Spectrometer
Imikorere | |
Imbaraga | 220V, 50Hz |
Ubushyuhe | 15 ℃ -35 ℃ |
Ubushuhe | 25% -80% RH |
Ibisobanuro | |
Chromatografi | |
Ubushyuhe bw'itanura | Ubushyuhe bwo mucyumba + 10 ℃ -400 ℃ |
Ubushyuhe butajegajega | ≤ ± 0.03 ℃ |
Igipimo ntarengwa cyo gushyushya | 40 ℃ / min |
Igihe ntarengwa cyo gukora | 999.99 min |
Ibice 10 byateganijwe kugenzura ubushyuhe | |
Gutandukanya / gutandukanya ibice (igisekuru cya 3 EPC) | |
Ubushyuhe ntarengwa: 400 ℃ | |
Umuvuduko ukoreshwa na elegitoronike, umuvuduko wikigereranyo no gutandukana | |
Urwego rwumuvuduko: 0-999 kPa | |
Urwego rutemba: 0-200 mL / min | |
Autosampler (bidashoboka) | |
Imashini ya Mass | |
Ibisobanuro nyamukuru | |
Urutonde rusange | 1.5-1024.0 amu |
Umutekano rusange | Biruta 0.1 amu / 48 h |
Umwanzuro | Igice cya misa |
Ibyiyumvo | DB-5MS 30m * 0.25mm * 0.25um ya silika capillary inkingi cyangwa inkingi isa. Inkomoko ya EI, scan yuzuye: (intera 100-300 amu). 1 pg OFN S / N≥100: 1 |
Igipimo ntarengwa cyo gusikana | 10,000 amu / s |
Urwego rudasanzwe | 105 |
Inkomoko ya Ion | Ingaruka ya elegitoronike inkomoko (EI), bisanzwe. Inkomoko yimiti (CI), birashoboka. |
Amashusho abiri | Porogaramu ishobora guhinduka |
Ikirangantego ntarengwa | 3 A. |
Ibyuka bihumanya ikirere | 10 - 350μA irashobora guhinduka |
Ingufu za Ionisation | 5 - 150eV irashobora guhinduka |
Ubushyuhe bwa Ion | 150 - 320 ℃ guhinduka, kugenzurwa kugiti cyawe |
Isesengura rusange | Quadrupole. Gusikana byuzuye, guhitamo ion ikurikirana (SIM) no kugura. Hafi ya matsinda 128 muburyo bwa SIM. Hafi ya 128 ion muri buri tsinda. |
Detector | kugwiza electron + imbaraga nyinshi dynode inyuma yibanda kumateraniro |
Imigaragarire ya GC-MS | |
Kugenzurwa kugiti cyawe binyuze mumashanyarazi, 150 - 320 ℃ birashobora guhinduka | |
Sisitemu ya Vacuum | |
Pompe ya Turbo (250 L / s), pompe ya mashini (180 L / min) | |
Urwego rwagutse rwuzuye ubukonje bwa cathode | |
Sisitemu yo gutunganya amakuru | |
Ibyuma | Mudasobwa (bidashoboka) |
Mucapyi | Icapa rya Laser (bidashoboka) |
Porogaramu | MS3200RT Porogaramu nyayo yo kubona amakuru hamwe no gutunganya amakuru ya MS3200P Porogaramu |
Ibikoresho bidahitamo | |
DIP 100 isukari / ikomeye iterwa inshinge | |
Igikoresho cya Thermal desorption | |
Dynamic headspace sampler | |
Gukuramo-no-umutego icyitegererezo |
Design Igishushanyo mbonera gishya, cyoroshye kandi gitanga ubuntu, kidasanzwe kandi kigizwe na GC igenzura.Igishushanyo mbonera kireba kurinda amakosa yukoresha.
Control Igenzura rya gazi ya EPC ryemera igisekuru cya gatatu EPC igenzurwa na sosiyete yacu, hamwe nigitutu cyangwa uburyo bwo kugenzura ibintu.Isuku ya valve igenzurwa hakoreshejwe uburyo bwa elegitoronike kugirango igabanye urugero rwo gukwirakwiza no gutakaza.Gutandukanya / gutandukanya uburyo bwo gutera inshinge birashobora kuzuza ibisabwa bitandukanye.Igikorwa cyo kubika ikirere cyikora kigabanya neza ikiguzi cyo gukora.Umwimerere uhita uhinduranya tekinoroji idafite amajwi apfuye ikuraho igihe kirekire cyo gutegereza igitutu gihamye mugihe icyerekezo cya valve gifunguye muburyo bwo gutandukanya inshinge.Ibi bitezimbere neza imiterere yimpera no gusubiramo igihe cyo kugumana.
Sisitemu yo kugenzura ubushyuhe bwa GC butezimbere uburyo bwo kugenzura ubushyuhe bwamashyiga kuri ± 0.03 ℃, butezimbere gusubiramo.Imyanya yubatswe ya azote, hydrogène hamwe na gaze ya gazi yo mu kirere irashobora guhuzwa nibindi bikoresho bya chromatografique ukurikije ibyo abakoresha bakeneye.Gusubiramo gahunda yubushyuhe byatejwe imbere, bivamo impagarike ikaze yibintu byinshi mumavuta.
Mod Igikoresho cyihariye cya CI reagent igenzura uburyo bwo kugenzura ibitekerezo, bihita bihindura umuvuduko wa gazi ya reagent kugera kurwego rwiza ugereranije na gaze ya gaze ya CI, bityo bikabika gaze ya reagent mugihe byemeza ko isesengura rya CI risubirwamo cyane.
◆ Byoroheje kandi bifatika byamazi meza kandi akomeye yo gutera inshinge zirashobora gukora isesengura ryihuse ryimiterere yibintu bitazwi, bitanga igikoresho gikomeye cyo gukoresha imiti ikoreshwa.Ubushyuhe budasanzwe bushobora gushyirwaho biroroshye kubisimbuza mugihe byangiritse cyangwa byanduye.Ubushyuhe bwo hejuru ni 650 ° C.
Bihujwe nibisanzwe GC inkingi.
Aut Autosampler.
Can Porogaramu irashobora gushyirwaho hamwe nibikoresho bitandukanye bya periferique.Gukuraho no gutega umutego, autosampler yamazi, desorption yumuriro, umutwe wumutwe, nibindi birashobora gushirwaho byoroshye, kugenwa no kugenzurwa.Icyongeweho DO (isohoka rya digitale) icyambu kirashobora gukoreshwa mugucunga ibikoresho byo hanze
Aut Udushya twa rotatable fluid autosampler irashobora kuzunguruka 360 ° hejuru ya horizontal.Autosampler irashobora gukurwa muburyo bworoshye kugirango uyorohereze GC.
Sisitemu ikomeye ya software:
Umukoresha wa gicuti ya software itanga ubworoherane bwo gukoresha hamwe nibikoresho byinshi biranga abakoresha bateye imbere.MS3200RT & MS3000P itanga ibisubizo bifatika kandi byoroshye kubakoresha ibyo bakeneye.
MS3200RT Kwishakira amakuru no kugenzura
◆ Chromatogrammes, mass spectra, ibipimo nibikoresho byerekanwa icyarimwe muburyo busukuye.Abakoresha barashobora kwerekana amakuru yose yingirakamaro mugihe cyo gusesengura.
Mod Uburyo bwo gusikana buboneka burimo Gusikana, guhitamo ion ikurikirana (SIM), cyangwa guhinduranya Scan na SIM.Hitamo uburyo bwo gusikana ukurikije umuvuduko wisesengura wifuza.
Ibipimo byose byisesengura birashobora kugenzurwa hifashishijwe porogaramu, harimo gazi itwara, umuvuduko, ubushyuhe bwinkingi, ubushyuhe bwinjira, nibindi.
Method Uburyo bwo gusesengura burashobora koherezwa hanze no gutumizwa mu mahanga.
Ibipimo byimiterere yibikoresho byerekanwe mugihe nyacyo.Impuruza zerekanwa mumabara agaragara.Imikorere yo gukingira ibyuma byikora birinda ibice byoroshye nka filament, detector, nibindi.
◆ Igiteranyo cya ion chromatogramu hamwe na sprifike ya misa irerekanwa muburyo bumwe kugirango yemererwe kugereranya byoroshye.Mass spectran irashobora kwerekanwa nkigishushanyo mbonera cyatunganijwe cyangwa nkamakuru yibanze.
Snap Snap spekrifisiyo yo kwimura imikorere imwe kanda itumiza dosiye-nyayo muri software itunganya amakuru kugirango isesengure ryuzuye kandi ryinshi.
Software Porogaramu itanga imikorere isanzwe kubakoresha bashya.Abakoresha bateye imbere barashobora gukoresha urufunguzo rwihuta kugirango bagere kubintu byihuse.Tangira, uhagarare, nibindi bikorwa birashobora gukorwa ukoresheje buto igerwaho kumurongo wingenzi.
◆ Byombi intoki na automatic mass specting tuning yatanzwe.Imiterere yo guhuza ikubiyemo gukemura, kumva, kugereranya ubwinshi, nibindi.Ibi birashobora gushyirwaho ukurikije ibisabwa.Muburyo bwo guhuza intoki, ingaruka zimpinduka zose mubipimo byerekana ibimenyetso rusange birashobora kugaragara.Guhuza intoki birakwiriye kubisabwa bidasanzwe hamwe nabakoresha bafite amateka akomeye muri rusange.Ibipimo hamwe na misa byerekanwe hamwe kugirango byoroshye kwitegereza.
◆ Porogaramu irashobora gukora vacuum igenzura imikorere, ningirakamaro mugutunganya ibikoresho.
Status Imiterere y'ibikoresho irashobora gukurikiranwa muguhuza ibice kugirango urinde igikoresho.
Hindura hagati ya EI (electron ionisation) na CI (ionisiyonike ya chimique).Zimya / kuzimya ibice.
Reporting Guhuza raporo birashobora gucapurwa vuba nyuma yo gutunganya birangiye.
Imikorere yo gusuzuma ibikoresho bya kure itanga ubufasha bwihuse kandi bwumwuga kubikoresho byawe aho ariho hose kwisi.
Porogaramu yo gutunganya amakuru ya MS3200P
Methods Uburyo bwose bwo gutunganya amakuru buratangwa.Igiteranyo cya ion chromatogramu (TIC), icyerekezo rusange, ion imwe ya chromatogramu (MC), ion chromatogramu nyinshi (MIC) irerekanwa kuri ecran imwe kugirango imenyekane byoroshye no kugereranya ubuziranenge bwimpinga.
◆ Kubisesengura byujuje ubuziranenge, umubare wibintu bisa bigaragara muri raporo yujuje ubuziranenge urashobora gushyirwaho ukurikije ibisabwa.Raporo yibirimo irashobora gushyirwaho kugirango ubone raporo yoroheje yujuje ubuziranenge.
Functions Imikorere ihagije ikubiyemo uburyo busanzwe, uburyo bwimbere bwimbere, uburyo busanzwe nuburyo bukosowe.MC, TIC, MIC byose birashobora guhurizwa hamwe no kubarwa.
Function Imikorere itatu-yerekana imikorere yerekana igihe cyo kugumana, ubukana, numubare rusange muburyo bwimbitse muri sisitemu imwe yo guhuza ibikorwa.
Software Porogaramu ya MS3200 MS izanye ibikoresho bya peteroli byabigize umwuga byo gusesengura byihuse ibikomoka kuri peteroli kugirango bigenzurwe neza.Ibiranga harimo kubara spekiteri, guhuza itsinda ryerekanwe hamwe nitsinda ryoherejwe hanze.Igikoresho cyo kubara SNR gifasha gusuzuma imikorere yibikoresho igihe icyo aricyo cyose.Imikorere ya spekrice yongeyeho nogukuramo ikoreshwa mugukosora inzitizi zatewe nurusaku rwa sisitemu.
File Amadosiye yamakuru yoherejwe muburyo bwa CDF kandi arashobora gutumizwa mubindi software.
◆ Ibindi bice birimo imiterere yerekana neza, uburyo bworoshye bwo guhuza impinga, ubushobozi bukomeye bwo gutunganya hamwe nuburyo bwuzuye bwo kubara
Library Isomero risanzwe ryerekana isomero ritanga intoki imwe yibibazo, hamwe nibibazo.Umukoresha asobanura amasomero arashobora gukoreshwa mubikorwa bidasanzwe.
Imikorere myiza ya GC-MS 3200 ituma ikoreshwa mubikorwa bitandukanye birimo umutekano wibiribwa, umutekano wibidukikije, imiti, nibindi.
Kumenya Melamine mu mata
Gusesengura ibinyabuzima bihindagurika (VOC) mumazi yo kunywa cyangwa Amazi yo hejuru
Kumenya Plastiseri muri Liquors
Kurikirana PAHs Kumenya
Kumenya imiti yica udukoko twa Organochlorine
Analysis Isesengura ryihuse rya Semi-quantitale ya Hydrocarbone
Analysis Isesengura ryuzuye ryintangarugero zitamenyekanye ukoresheje Injection itaziguye
Ibishushanyo bikurikira birakoreshwa mugupima ubuziranenge bwamazi
(bikurikizwa muburyo bwa EPA 502.2)
Isesengura n'umutego wisesengura + GC-MS 3200 + MS3200 paki ya software + DB-624 (30 m × 0,25 mm × 1.4 μ m) yahujwe na silika capillary inkingi
Umwanya wa sampler + GC-MS 3200 + Porogaramu ya software ya MS3200 + DB-624 (30 m × 0,25 mm × 1.4 μ m) yahujwe na silika capillary inkingi
Bikoreshwa muburyo bwo kumenya ibinyabuzima bihindagurika mumazi yo hejuru, amazi yo kunywa n'amazi y'ibigega.
Configuration Imiterere yubukungu ikoreshwa mugukurikirana ikirere cyiza
EW-3TD igikoresho cya desorption yamashanyarazi + GC-MS 3200+ paki ya software ya MS3200 + ihwanye na DB-5MS inkingi (30 mx 0,25 mm x 0,25 μ m) inkingi iringaniye
Birakoreshwa mukugerageza ubuziranenge bwikirere mubidukikije no mumwanya rusange.Itanga ibyiyumvo byinshi kuri TVOC hamwe nizindi myuka yangiza.
Configuration Ibisanzwe bisanzwe bikoreshwa mubisesengura rya laboratoire
Autosampler + GC-MS 3200 + MS3200 pack ya software + DB-5MS (30m × 0.25mm × 0.25μm) yahujwe na silika capillary inkingi
Birakwiriye gusesengura ubuziranenge nubunini bwibintu byinshi kama nkibirungo na parufe, imiti yica udukoko, isesengura ryicyitegererezo cya PAHs.
Iboneza bikurikizwa kugenzura ubuziranenge muburyo bwa synthesis
DIP100 + GC-MS 3200+ Porogaramu ya software ya MS3200 + DB-5MS (30m × 0.25mm × 0.25μm) yahujwe na silika capillary inkingi
Birakoreshwa muburyo bwihuse bwo gusesengura imiti ihuza imiti hamwe nibicuruzwa byanyuma hamwe nisesengura ryinshi hamwe na GC intangiriro.
Laboratoire igendanwa yashyizwe mu modoka ikurikirana
Laboratoire yisesengura irashobora gushirwa kumurongo wa laboratoire igendanwa kugirango hakorwe iperereza ryihuse ryangiza imiti mugihe habaye ibiribwa byangiza ibidukikije.